tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

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Chemical Name:tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate
CAS No.:1391999-72-6
Molecular Formula:C₃₅H₄₈N₂O₁₀
Molecular Weight:656.774
Hs Code.:

Synonyms:tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

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Chemical Property of tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

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Technology Process of tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

There total 12 articles about tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1391999-71-5
tert-butyl 2-(2-isocyanato-3-isopropoxyphenoxy)acetate

: 1391999-67-9
tert-butyl 2-(3-(allylcarbamoyl)-5-isopropoxyphenoxy)acetate

: 1391999-72-6
tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

Guidance literature:: tert-butyl 2-(3-(allylcarbamoyl)-5-isopropoxyphenoxy)acetate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.25h; Inert atmosphere;

tert-butyl 2-(2-isocyanato-3-isopropoxyphenoxy)acetate; With acetic acid; In tetrahydrofuran; toluene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c2ob25273b

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1391999-72-6
tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 90 °C / Inert atmosphere

2.1: 5%-palladium/activated carbon; hydrogen / ethanol / 12 h / Inert atmosphere

3.1: sodium hydrogencarbonate / dichloromethane; water / 0.67 h / 20 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2ob25273b

Reference yield:

: C₁₆H₂₁ClO₅

: 1391999-72-6
tert-butyl 2-(3-(allyl((2-(2-(tert-butoxy)-2-oxoethoxy)-6-isopropoxyphenyl)carbamoyl)carbamoyl)-5-isopropoxyphenoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

With potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2ob25273b