p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

Base Information

Chemical Name:p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside
CAS No.:1602921-31-2
Molecular Formula:C₃₁H₃₂O₄S
Molecular Weight:500.659
Hs Code.:

Synonyms:p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

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Technology Process of p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

There total 3 articles about p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₃₁H₃₀O₄S

: 1602921-31-2
p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; at -20 - 20 ℃; for 3h;
DOI:10.1002/ejoc.201400006

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1602921-31-2
p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

2: boron trifluoride diethyl etherate; trimethylsilyl trifluoromethanesulfonate / 3 h / -20 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/ejoc.201400006

Reference yield:

: p-methylphenyl 4,6-O-benzylidene-2-deoxy-1-thio-D-glucopyranoside

: 1602921-31-2
p-tolyl 4-O-benzyl-3-O-(2-naphthylmethyl)-2-deoxy-1-thio-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

2: boron trifluoride diethyl etherate; trimethylsilyl trifluoromethanesulfonate / 3 h / -20 - 20 °C

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/ejoc.201400006