di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate)

Base Information

• Chemical Name: di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate)
• CAS No.: 1490389-71-3
• Molecular Formula: C₄₆H₇₄N₄O₈
• Molecular Weight: 811.116

Synonyms:di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate)

Chemical Property of di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate)

Chemical Property:

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Technology Process of di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate)

There total 1 articles about di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

4-Methoxyphenylacetic acid (104-01-8) + N1,N12-di(tert-butyloxycarbonyl)-N1,N12-di(3-aminopropyl)-1,12-dodecanediamine (336881-11-9) → di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate) (1490389-71-3)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 23h; Inert atmosphere;

DOI:10.1016/j.ejmech.2013.07.055

Reference yield: 96.0%

di-tert-butyl dodecane-1,12-diylbis(3-(2-(4-methoxyphenyl)acetamido)propylcarbamate) (1490389-71-3) + trifluoroacetic acid (76-05-1) → N1,N12-bis(3-(2-(4-methoxyphenyl)acetamido)propyl)dodecane-1,12-diaminium 2,2,2-trifluoroacetate

Guidance literature:

In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.ejmech.2013.07.055

upstream raw materials:

4-Methoxyphenylacetic acid

N¹,N¹²-di(tert-butyloxycarbonyl)-N¹,N¹²-di(3-aminopropyl)-1,12-dodecanediamine

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