(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

Base Information

Chemical Name:(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide
CAS No.:128113-65-5
Molecular Formula:BrH*C₂₁H₂₉NO₃
Molecular Weight:424.378
Hs Code.:

Synonyms:(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

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Chemical Property of (1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

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Technology Process of (1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

There total 3 articles about (1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: [1-(2-Isopropoxy-3,4-dimethoxy-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

: 128113-65-5
(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

Guidance literature:: With hydrogen; nickel; In ethanol; under 3750.3 Torr;
DOI:10.1016/S0040-4039(00)95189-X

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 128113-65-5
(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄, Et₃N / CH₂Cl₂

2: 74 percent / H₂ / Raney-Ni / ethanol / 3750.3 Torr

With hydrogen; titanium tetrachloride; triethylamine; nickel; In ethanol; dichloromethane;
DOI:10.1016/S0040-4039(00)95189-X

Reference yield:

: 128113-84-8
1-(2-isopropoxy-3,4-dimethoxyphenyl)-1-ethanone

: 128113-65-5
(1S,1'S)-N-(1'-phenylethyl)-1-(2''-isopropoxy-3'',4''-dimethoxyphenyl)ethylamine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄, Et₃N / CH₂Cl₂

2: 74 percent / H₂ / Raney-Ni / ethanol / 3750.3 Torr

With hydrogen; titanium tetrachloride; triethylamine; nickel; In ethanol; dichloromethane;
DOI:10.1016/S0040-4039(00)95189-X