4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol

Base Information

• Chemical Name: 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol
• CAS No.: 1241948-94-6
• Molecular Formula: C₂₇H₃₁NO₄
• Molecular Weight: 433.547

Synonyms:4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol

Chemical Property of 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol

Chemical Property:

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Technology Process of 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol

There total 1 articles about 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

pentyl 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)benzoate (1241948-93-5) → 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol (1241948-94-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 25 ℃;

DOI:10.1021/jo1009849

Reference yield: 89.0%

4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol (1241948-94-6) + ethyl 4-hydroxy-3-nitrobenzoate (19013-10-6) → ethyl 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)benzyloxy)-3-nitrobenzoate (1241948-96-8)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/jo1009849

Reference yield: 48.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol (1241948-94-6) → 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol 4-nitrophenyl ether (1241948-95-7)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/jo1009849

upstream raw materials:

pentyl 4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)benzoate

Downstream raw materials:

4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)-benzyl alcohol 4-nitrophenyl ether

ethyl 4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-(N-benzyl-N-ethylamino)benzyloxy)-3-nitrobenzoate

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