C₂₇H₃₀N₂O₇S

Base Information

Chemical Name:C₂₇H₃₀N₂O₇S
CAS No.:1094172-76-5
Molecular Formula:C₂₇H₃₀N₂O₇S
Molecular Weight:526.61
Hs Code.:

C<sub>27</sub>H<sub>30</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₇H₃₀N₂O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₀N₂O₇S

Chemical Property:

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Technology Process of C₂₇H₃₀N₂O₇S

There total 9 articles about C₂₇H₃₀N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1094172-67-4
C₃₆H₅₀N₂O₇SSi

: 1094172-76-5
C₂₇H₃₀N₂O₇S

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; water; at 0 ℃; for 0.333333h;
DOI:10.1002/ejoc.201100242

Reference yield:

: C₁₃H₁₅BrN₂O₃

: 1094172-76-5
C₂₇H₃₀N₂O₇S

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C

2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C

3: dmap; triethylamine / toluene / 18 h / 70 °C

4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

5: dichloromethane / 4 h / 20 °C

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

With dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; magnesium sulfate; acetic acid; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile; 6: Sonogashira coupling;
DOI:10.1002/ejoc.201100242

Reference yield:

: 1094172-65-2
C₂₀H₂₁BrN₂O₄

: 1094172-76-5
C₂₇H₃₀N₂O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / toluene / 18 h / 70 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

3: dichloromethane / 4 h / 20 °C

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

With dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile; 4: Sonogashira coupling;
DOI:10.1002/ejoc.201100242