C₁₈H₁₄ClN₃O₃S₂

Base Information

Chemical Name:C₁₈H₁₄ClN₃O₃S₂
CAS No.:1329991-72-1
Molecular Formula:C₁₈H₁₄ClN₃O₃S₂
Molecular Weight:419.912
Hs Code.:

C<sub>18</sub>H<sub>14</sub>ClN<sub>3</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:C₁₈H₁₄ClN₃O₃S₂

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Chemical Property of C₁₈H₁₄ClN₃O₃S₂

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Technology Process of C₁₈H₁₄ClN₃O₃S₂

There total 8 articles about C₁₈H₁₄ClN₃O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329991-71-0
C₁₈H₁₄ClN₃OS₂

: 1329991-72-1
C₁₈H₁₄ClN₃O₃S₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 0.75h; Reflux;

Reference yield:

: 39736-29-3
ethyl 4-amino-2-(methylthio)thiazol-5-carboxylate

: 1329991-72-1
C₁₈H₁₄ClN₃O₃S₂

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / dichloromethane / 1.25 h / 20 °C / Cooling with ice; Inert atmosphere

2: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 3.25 h / 0 - 20 °C

3: potassium carbonate; ethanol / 1 h / Reflux

4: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

5: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 6 h / 20 °C

6: sodium hydride / pyridine; oil / 3 h / 50 °C / Cooling with ice

7: triethylamine / copper diacetate / dichloromethane / 1 h / Reflux

8: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.75 h / Reflux

With pyridine; ethanol; hydrogen; sodium hexamethyldisilazane; sodium hydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; palladium 10% on activated carbon; copper diacetate; In tetrahydrofuran; pyridine; dichloromethane; chloroform; isopropyl alcohol; oil;

Reference yield:

: 1329991-66-3
C₁₀H₁₁F₃N₂O₃S₂

: 1329991-72-1
C₁₈H₁₄ClN₃O₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; ethanol / 1 h / Reflux

2: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere

3: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 6 h / 20 °C

4: sodium hydride / pyridine; oil / 3 h / 50 °C / Cooling with ice

5: triethylamine / copper diacetate / dichloromethane / 1 h / Reflux

6: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.75 h / Reflux

With ethanol; hydrogen; sodium hexamethyldisilazane; sodium hydride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; copper diacetate; In tetrahydrofuran; pyridine; dichloromethane; chloroform; isopropyl alcohol; oil;