[(4-Iodophenyl)methyl]hydrazine

Base Information

• Chemical Name: [(4-Iodophenyl)methyl]hydrazine
• CAS No.: 51859-97-3
• Molecular Formula: C₇H₉IN₂
• Molecular Weight: 248.066
• DSSTox Substance ID: DTXSID90606212
• Wikidata: Q82504860

Synonyms:[(4-Iodophenyl)methyl]hydrazine;51859-97-3;(4-Iodobenzyl)hydrazine;(4-iodophenyl)methylhydrazine;p-iodobenzylhydrazine;SCHEMBL11619172;DTXSID90606212;JRBYEYSVCBDBQO-UHFFFAOYSA-N

Chemical Property of [(4-Iodophenyl)methyl]hydrazine

Chemical Property:

• XLogP3: 1.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 247.98105
• Heavy Atom Count: 10
• Complexity: 89.6

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1CNN)I

Technology Process of [(4-Iodophenyl)methyl]hydrazine

There total 1 articles about [(4-Iodophenyl)methyl]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromomethyl-4-iodobenzene (16004-15-2) → 4-iodobenzyl-hydrazine (51859-97-3)

Guidance literature:

With hydrazine hydrate; In ethanol; at 0 - 20 ℃;

DOI:10.1021/jm070680h

Reference yield: 15.0%

4-iodobenzyl-hydrazine (51859-97-3) + (S)-2-(methoxycarbonylamino)-3,3-dimethylbutanoic acid (162537-11-3) → {(S)-1-[N'-(4-iodobenzyl)hydrazinocarbonyl]-2,2-dimethylpropyl}carbamic acid methyl ester (1010702-58-5)

Guidance literature:

With benzotriazol-1-ol; In dichloromethane; at 20 ℃;

DOI:10.1021/jm070680h

Reference yield:

4-iodobenzyl-hydrazine (51859-97-3) + β-amino-β-ethoxyacrylic acid ethyl ester (119180-07-3) → 3-Amino-1-(4-iodobenzyl)-pyrazol-5-one

Guidance literature:

With toluene-4-sulfonic acid; In ethanol;

upstream raw materials:

1-bromomethyl-4-iodobenzene

Downstream raw materials:

{(S)-1-[N'-(4-iodobenzyl)hydrazinocarbonyl]-2,2-dimethylpropyl}carbamic acid methyl ester

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