[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

Base Information

Chemical Name:[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate
CAS No.:1439366-77-4
Molecular Formula:C₁₈H₂₃NO₅
Molecular Weight:333.384
Hs Code.:

Synonyms:[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

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Chemical Property of [3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

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Technology Process of [3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

There total 4 articles about [3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 1659-31-0
2,2'-dipyridyl carbonate

: 1237534-99-4
(3R,4S)-2-methyl-4-oxo-3-oxetanylammonium toluene-4-sulfonate

: 1439367-59-5
3-(4-phenylbutyl)-oxetan-3-ol

: 1439366-77-4
[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

Guidance literature:: 2,2'-dipyridyl carbonate; 3-(4-phenylbutyl)-oxetan-3-ol; With triethylamine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

(3R,4S)-2-methyl-4-oxo-3-oxetanylammonium toluene-4-sulfonate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/jm501455s

Reference yield:

: 1439367-61-9
[3-(4-phenylbutyl)-oxetan-3-yl] 2-oxopyridine-1-carboxylate

: 131131-06-1
(3S,4R)-2-methyl-4-oxo-3-oxetanylammonium toluene-4-sulfonate

: 1439366-77-4
[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

Reference yield:

: 13633-25-5
1-Bromo-4-phenylbutane

: 1439366-77-4
[3-(4-phenylbutyl)oxetan-3-yl] N-[(2S,3R)-2-methyl-4-oxo-oxetan-3-yl]-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium / diethyl ether / 3 h / -45 - 0 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

2.1: dmap / dichloromethane / 17 h / 20 °C / Inert atmosphere

2.2: 15 h / 20 °C / Inert atmosphere

With dmap; lithium; In diethyl ether; dichloromethane;