10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide

Base Information

• Chemical Name: 10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide
• CAS No.: 955938-07-5
• Molecular Formula: C₅₈H₇₀N₁₀O₅
• Molecular Weight: 987.258

Synonyms:10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide

Chemical Property of 10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide

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Technology Process of 10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide

There total 1 articles about 10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N⁽¹⁾,N⁽⁴⁾,N⁽⁷⁾-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

6-(tert-butyl)-2-[3-(1,4,7,10-tetraazacyclododec-1-ylmethyl)-1H-pyrazol-1-yl]-10H-9-oxa-1-azaanthracen-10-one + 2-chloro-N-((1S)-1-phenylethyl)acetamide (36293-01-3) → 10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N(1),N(4),N(7)-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide (955938-07-5)

Guidance literature:

With caesium carbonate; potassium iodide; In acetonitrile; for 16h; Heating / reflux;

Reference yield: 69.0%

10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N(1),N(4),N(7)-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide (955938-07-5) + terbium(III) trifluoromethanesulfonate → (10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N(1),N(4),N(7)-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide)terbium(III) tris(trifluoromethanesulfonate)

Guidance literature:

In acetonitrile; for 16h; Heating / reflux;

Reference yield: 69.0%

10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N(1),N(4),N(7)-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide (955938-07-5) + terbium(III) trifluoromethanesulfonate hexahydrate → (10-((1-[6-(tert-butyl)-10-oxo-10H-9-oxa-1-azaanthracen-2-yl]-1H-pyrazol-3-yl)methyl)-N(1),N(4),N(7)-tris[(1S)-1-phenylethyl]-1,4,7,10-tetraazacyclododecane-1,4,7-triacetamide)terbium(III) trichloride

Guidance literature:

In acetonitrile; CH₂Cl₂; soln. of Tb salt and ligand in MeCN refluxed under Ar for 18 h, evapn., CH2Cl2 added to residue, mixt. sonicated for 10 min, decantation, solid dissolved in MeCN, added slowly onto Et2O, ppt. stirred in H2O contg. Dowex-Cl resin at room temp. for 3 h; resin filtered off, filtrate concd.;

DOI:10.1002/hlca.200900122

upstream raw materials:

2-chloro-N-((1S)-1-phenylethyl)acetamide

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