PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

Base Information

Chemical Name:PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)
CAS No.:618384-77-3
Molecular Formula:C₂₄H₂₉ClNPPt
Molecular Weight:593.008
Hs Code.:

Synonyms:PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

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Chemical Property of PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

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Technology Process of PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

There total 1 articles about PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: Pt(1,5-cyclooctadiene)(Ph)(Cl)

: 2359-97-9
2-(diphenylphosphino)triethylamine

: 618384-77-3
PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

Guidance literature:: In benzene; under inert atm. Et2NCH2CH2PPh2 was added to benzene soln. PtPhCl(cod) and stirred for 1 h at room temp.; ppt. was filtered, washed with hexane and recrystd. from CH2Cl2 at -30°C; elem. anal.;
DOI:10.1021/om030477u

Reference yield: 90.0%

: 12107-36-7
sodium(η5-cyclopentadienyl)tricarbonyltungstate(II)

: 618384-77-3
PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

: silver nitrate

: (2-(diphenylphosphino)triethylamine-κ(2)N,P)PhPt-WCp(CO)3

: silver(I) chloride

Guidance literature:: With AgNO₃; In tetrahydrofuran; byproducts: AgCl; under inert atm. Pt complex and AgNO3 were dissolved in THF and stirred overnight at room temp., ppt. was filtered off, filtrate was added to THF soln. Na(WCp(CO)3) at -70°C, react. mixt. was stirred for 3 h at -30°C; volatiles were evapd., residue was extd. with toluene at -20°C, soln. was filtered and concd. under reduced pressure at -20°C, hexane was added, ppt. was filtered, washed with hexane, and dried under vac. at room temp.; elem. anal.;
DOI:10.1021/om030477u

Reference yield: 77.0%

: 12107-35-6
Na[CpMo(CO)3]

: 618384-77-3
PtPhCl(2-(ddiphenylphosphino)triethylamine-κ2N,P)

: silver nitrate

: (2-(diphenylphosphino)triethylamine-κ(2)N,P)PhPt-MoCp(CO)3

: silver(I) chloride

Guidance literature:: With AgNO₃; In tetrahydrofuran; byproducts: AgCl; under inert atm. Pt complex and AgNO3 were dissolved in THF and stirred overnight at room temp., ppt. was filtered off, filtrate was added to THF soln. Na(MoCp(CO)3) at -70°C, react. mixt. was stirred for 3 h at -30°C; volatiles were evapd., residue was extd. with toluene at -20°C, soln. was filtered and concd. under reduced pressure at -20°C, hexane was added, ppt. was filtered, washed with hexane, and dried under vac. at room temp.; elem. anal.;
DOI:10.1021/om030477u