3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

Base Information

Chemical Name:3,5-diethynylphenol dibenzo[24]crown-8-carboxylate
CAS No.:1020182-77-7
Molecular Formula:C₃₅H₃₆O₁₀
Molecular Weight:616.665
Hs Code.:

Synonyms:3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

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Technology Process of 3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

There total 1 articles about 3,5-diethynylphenol dibenzo[24]crown-8-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 215322-83-1
2,5,8,11,18,21,24,27-octaoxa-tricyclo[26.4.0.0^12,17]dotriaconta-1⁽²⁸⁾,12,14,16,29,31-hexaene-14-carboxylic acid

: 918826-08-1
3,5-diethynyl-phenol

: 1020182-77-7
3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1021/ja711502t

Reference yield: 65.0%

: 35084-99-2,15692-97-4,15636-79-0
trans diiodobis(triethylphosphine)platinum(II)

: 1020182-77-7
3,5-diethynylphenol dibenzo[24]crown-8-carboxylate

: 1020182-78-8
Pt₂I₂(3,5-diethynylphenol dibenzo[24]crown-8 carboxylate(-2H))(triethylphosphine)4

Guidance literature:: With copper(l) iodide; In toluene; byproducts: (CH3CH2)2NH2I; addn. of toluene and amine deriv. to mixt. of platinum compd. and crown ether deriv. under N2, stirring at room temp. for 10 min, addn. of copper compd., keeping at room temp. for 16 h; evapn., chromy. (silica gel, CH2Cl2/acetone (5:1)), elem. anal.;
DOI:10.1021/ja711502t