allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

Base Information

Chemical Name:allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside
CAS No.:1360605-67-9
Molecular Formula:C₂₁H₂₆Cl₃NO₈
Molecular Weight:526.798
Hs Code.:

Synonyms:allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

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Technology Process of allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

There total 2 articles about allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63064-49-3,65947-37-7,74984-84-2,88903-98-4,92841-84-4,116347-88-7,136845-44-8,138456-61-8,74984-83-1
allyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 1360605-67-9
allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

2: sodium cyanoborohydride / tetrahydrofuran / 2 h / Molecular sieve; Inert atmosphere

With pyridine; sodium cyanoborohydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201101342

Reference yield:

: C₂₁H₂₄Cl₃NO₈

: 1360605-67-9
allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; for 2h; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1002/ejoc.201101342

Reference yield: 75.0%

: 178476-15-8
2,4,6-tri-O-acetyl-3-O-chloroacetyl-α-D-galactolpyranosyl trichloroacetimidate

: 1360605-67-9
allyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

: 1360605-71-5
allyl 2-acetamido-4-O-(2,4,6-tri-O-acetyl-3-O-chloroacetyl-β-D-galactopyranosyl)-6-O-benzyl-2-deoxy-3-O-trichloroethyloxylcarbonyl-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 40 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/ejoc.201101342