3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

Base Information

Chemical Name:3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid
CAS No.:160726-37-4
Molecular Formula:C₂₃H₂₄O₆
Molecular Weight:396.44
Hs Code.:

Synonyms:3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

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Chemical Property of 3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

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Technology Process of 3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

There total 4 articles about 3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 160726-36-3
3-<4-methoxy-3-<4-(3-methoxy-3-oxo-1-propenyl)-phenoxy>phenyl>-2-propenoic acid t-butyl ester

: 160726-37-4
3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

Guidance literature:: With sodium hydroxide; In 1,2-dimethoxyethane; for 0.333333h; Heating;

Reference yield:

: 129866-90-6
2,2'-dimethoxy-5,5'-diformyl-diphenyl-iodonium bromide

: 160726-37-4
3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaOMe / 1.) MeOH, 2.) DME, reflux, 72 h

2: 75 percent / piperidine / pyridine / 1.67 h / 100 °C

3: 95 percent / H₂SO₄ / CH₂Cl₂ / 6 h

4: 83 percent / 5percent aq. NaOH / 1,2-dimethoxy-ethane / 0.33 h / Heating

With piperidine; sodium hydroxide; sulfuric acid; sodium methylate; In pyridine; 1,2-dimethoxyethane; dichloromethane;

Reference yield:

: 160726-34-1
methyl 3-<4-(2-methoxy-5-formylphenoxy)-phenyl>-2-propenoate

: 160726-37-4
3-<4-<2-methoxy-5-(3-oxo-3-t-butoxy-1-propenyl)-phenoxy>phenyl>-2-propenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / piperidine / pyridine / 1.67 h / 100 °C

2: 95 percent / H₂SO₄ / CH₂Cl₂ / 6 h

3: 83 percent / 5percent aq. NaOH / 1,2-dimethoxy-ethane / 0.33 h / Heating

With piperidine; sodium hydroxide; sulfuric acid; In pyridine; 1,2-dimethoxyethane; dichloromethane;