(1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol

Base Information

Chemical Name:(1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol
CAS No.:113471-34-4
Molecular Formula:C₁₀H₁₅NO*C₁₁H₁₄O₃
Molecular Weight:359.466
Hs Code.:

Synonyms:(1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol

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Chemical Property of (1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol

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Technology Process of (1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol

There total 4 articles about (1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 100058-98-8,106924-58-7,113352-73-1,113429-13-3,113429-14-4
(+/-)-(2,3-endo)-3-(1-oxopropyl)bicyclo<2.2.1>hept-5-ene-2-carboxylic acid

: 113471-34-4
(1S,2R,3S,4R)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1R,2S)-2-methylamino-1-phenyl-propan-1-ol

Guidance literature:: In benzene; for 0.25h; Ambient temperature;
DOI:10.1021/ja00215a039

Reference yield: 48.0%

: 321-98-2,7009-81-6,90-83-5,6912-63-6
(1S,2R)-(+)-ephedrine

: 100058-98-8,106924-58-7,113352-73-1,113429-13-3,113429-14-4
(+/-)-(2,3-endo)-3-(1-oxopropyl)bicyclo<2.2.1>hept-5-ene-2-carboxylic acid

: 113471-34-4
(1R,2S,3R,4S)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1S,2R)-2-methylamino-1-phenyl-propan-1-ol

Guidance literature:: In benzene; for 0.25h; Ambient temperature;
DOI:10.1021/ja00215a039

Reference yield:

: 129-64-6
3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

: 113471-34-4
(1R,2S,3R,4S)-3-Propionyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid; compound with (1S,2R)-2-methylamino-1-phenyl-propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / hexane; CH₂Cl₂ / 1 h / -10 °C

2: 48 percent / benzene / 0.25 h / Ambient temperature

In hexane; dichloromethane; benzene;
DOI:10.1021/ja00215a039