<imino>triphenylphosphorane

Base Information

• Chemical Name: <imino>triphenylphosphorane
• CAS No.: 171414-55-4
• Molecular Formula: C₂₅H₃₄NPSi₂
• Molecular Weight: 435.696

Synonyms:<imino>triphenylphosphorane

Chemical Property of <imino>triphenylphosphorane

Chemical Property:

Purity/Quality:

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Technology Process of <imino>triphenylphosphorane

There total 1 articles about <imino>triphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(trimethylsilyl)methyl azide (134340-01-5) + triphenylphosphine (603-35-0) → <imino>triphenylphosphorane (171414-55-4) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 2h; Yield given. Yields of byproduct given;

DOI:10.1021/jo00124a011

Reference yield: 56.0%

phenyl isocyanate (103-71-9) + <imino>triphenylphosphorane (171414-55-4) → 1,3-Diphenylcarbodiimide (622-16-2) + Bis(trimethylsilyl)methyl isocyanate (171414-56-5) + N-Phenyl-N'-carbodiimide (171414-58-7)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1021/jo00124a011

Reference yield: 42.0%

trimetylsilylketene (4071-85-6) + <imino>triphenylphosphorane (171414-55-4) → (Trimethylsilyl)ketene N-imine (171414-77-0)

Guidance literature:

In diethyl ether; at 25 ℃;

DOI:10.1021/jo00124a011

upstream raw materials:

bis(trimethylsilyl)methyl azide

triphenylphosphine

Downstream raw materials:

(Trimethylsilyl)ketene N-imine

1,3-Diphenylcarbodiimide

Bis(trimethylsilyl)methyl isocyanate

N-Phenyl-N'-carbodiimide

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