2,5-diacetylcyclohexaneacetaldehyde

Base Information

Chemical Name:2,5-diacetylcyclohexaneacetaldehyde
CAS No.:86374-46-1
Molecular Formula:C₁₂H₁₈O₃
Molecular Weight:210.273
Hs Code.:

Synonyms:2,5-diacetylcyclohexaneacetaldehyde

Suppliers and Price of 2,5-diacetylcyclohexaneacetaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,5-diacetylcyclohexaneacetaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-diacetylcyclohexaneacetaldehyde

There total 11 articles about 2,5-diacetylcyclohexaneacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 86374-42-7
6-acetyl-1-hydroxy-1-methyl-3,4,4a,6,7,8,8a-octahydro-1H-2-benzopyran

: 86374-46-1
2,5-diacetylcyclohexaneacetaldehyde

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/ja00355a028

Reference yield:

: 86420-17-9
(1S,2S,4R)-2-Bicyclo[2.2.2]oct-5-en-2-yl-ethanol

: 86374-46-1
2,5-diacetylcyclohexaneacetaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / pyridine / Ambient temperature

2: 93 percent / sodium metaperiodate, ruthenium trichloride hydrate / acetone; H₂O / Ambient temperature

3: 95.7 percent / thionyl chloride, triethylamine / benzene / 3 h / Heating

4: 8.5 g / cuprous iodide / diethyl ether / -40 deg C -> room temperature

5: 59.1 percent / sodium hydroxide / H₂O; methanol / 1 h / Ambient temperature

6: 85 percent / chromium trioxide, pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; chromium(VI) oxide; ruthenium trichloride; sodium hydroxide; sodium periodate; copper(l) iodide; thionyl chloride; triethylamine; In pyridine; methanol; diethyl ether; dichloromethane; water; acetone; benzene;
DOI:10.1021/ja00355a028

Reference yield:

: 86374-39-2
2-(2-acetoxyethyl)bicyclo<2.2.2>oct-5-ene

: 86374-46-1
2,5-diacetylcyclohexaneacetaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / sodium metaperiodate, ruthenium trichloride hydrate / acetone; H₂O / Ambient temperature

2: 95.7 percent / thionyl chloride, triethylamine / benzene / 3 h / Heating

3: 8.5 g / cuprous iodide / diethyl ether / -40 deg C -> room temperature

4: 59.1 percent / sodium hydroxide / H₂O; methanol / 1 h / Ambient temperature

5: 85 percent / chromium trioxide, pyridine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; chromium(VI) oxide; ruthenium trichloride; sodium hydroxide; sodium periodate; copper(l) iodide; thionyl chloride; triethylamine; In methanol; diethyl ether; dichloromethane; water; acetone; benzene;
DOI:10.1021/ja00355a028