N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide
CAS No.:787571-95-3
Molecular Formula:C₂₆H₂₉NO₅S
Molecular Weight:467.586
Hs Code.:

<i>N</i>-(3,4-dimethoxy-benzyl)-<i>N</i>-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

Synonyms:N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

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Chemical Property of N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

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Technology Process of N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

There total 6 articles about N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 787571-92-0
N-(3,5-dimethyl-4-hydroxyphenethyl)-N-tosyl-3,4-dimethoxybenzylamine

: 787571-95-3
N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

Guidance literature:: With silver(l) oxide; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/j.tetlet.2004.08.053

Reference yield:

: 168106-30-7
3,5-dimethyl-4-benzyloxy-phenyl acetic acid

: 787571-95-3
N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / H(+)

2: 75 percent / LAH

3: 76 percent / PPh₃; CBr₄

4: NaH / dimethylformamide

5: H₂ / Pd/C / ethyl acetate

6: Ag₂O / CH₂Cl₂ / 6 h / 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; hydrogen; hydrogen cation; sodium hydride; triphenylphosphine; silver(l) oxide; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2004.08.053

Reference yield:

: 787571-86-2
methyl 4-benzyloxy-3,5-dimethylphenylacetate

: 787571-95-3
N-(3,4-dimethoxy-benzyl)-N-[2-(3,5-dimethyl-4-oxo-cyclohexa-2,5-dienylidene)-ethyl]-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / LAH

2: 76 percent / PPh₃; CBr₄

3: NaH / dimethylformamide

4: H₂ / Pd/C / ethyl acetate

5: Ag₂O / CH₂Cl₂ / 6 h / 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; hydrogen; sodium hydride; triphenylphosphine; silver(l) oxide; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2004.08.053