7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

Base Information

Chemical Name:7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane
CAS No.:913300-20-6
Molecular Formula:C₁₉H₂₈O₂S₂
Molecular Weight:352.562
Hs Code.:

Synonyms:7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

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Technology Process of 7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

There total 1 articles about 7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913300-27-3
4-(2,3-dimethoxy-4-methylphenyl)-4,5,5-trimethylcyclopent-2-enone

: 913300-20-6
7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / hydrogen / Pd/C / ethanol / 1 h / 20 °C

2: 80 percent / iodine / CH₂Cl₂ / 0.5 h / 20 °C

With hydrogen; iodine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2006.07.062

Reference yield: 100.0%

: 913300-20-6
7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

: 913300-29-5
6-methyl-3-(1,2,2-trimethylcyclopentyl)benzene-1,2-diol dimethyl ester

Guidance literature:: With nickel; In ethanol; for 3h; Heating;
DOI:10.1016/j.tet.2006.07.062

Reference yield:

: 913300-20-6
7-(2,3-dimethoxy-4-methylphenyl)-6,7,7-trimethyl-1,4-dithiaspiro[4.4]nonane

: 159898-20-1
3-(1,2,2-trimethylcyclopentyl)-6-methylbenzene-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Raney nickel / ethanol / 3 h / Heating

2: 62 percent / boron tribromide / CH₂Cl₂ / 4 h / -40 °C

With boron tribromide; nickel; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2006.07.062