5-Allyloxy-2,4-dibenzoylphenol

Base Information

Chemical Name:5-Allyloxy-2,4-dibenzoylphenol
CAS No.:102593-73-7
Molecular Formula:C₂₃H₁₈O₄
Molecular Weight:358.394
Hs Code.:

Synonyms:5-Allyloxy-2,4-dibenzoylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Allyloxy-2,4-dibenzoylphenol

Chemical Property:

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Technology Process of 5-Allyloxy-2,4-dibenzoylphenol

There total 2 articles about 5-Allyloxy-2,4-dibenzoylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3088-15-1
4,6-dibenzoylresorcinol

: 106-95-6
allyl bromide

: 102593-73-7
5-Allyloxy-2,4-dibenzoylphenol

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃; for 12h; Reflux;
DOI:10.1021/acs.orglett.6b03865

Reference yield:

: 102593-73-7
5-Allyloxy-2,4-dibenzoylphenol

Guidance literature:: Allylbromid, entspr. Dihydroxyverb.;

Reference yield:

: 102593-73-7
5-Allyloxy-2,4-dibenzoylphenol

: ethyl-3-(5,7-dibenzoyl-4-hydroxy-2,3-dihydrobenzofuran-2-yl)-2,2-difluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 24 h / 180 °C / Inert atmosphere; Sealed tube

2: 1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate / 1,4-dioxane / 20 h / 80 °C / Sealed tube; Inert atmosphere; Schlenk technique

With 1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; In 1,4-dioxane;
DOI:10.1021/acs.orglett.6b03865