Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Base Information

Chemical Name:Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate
CAS No.:155099-10-8
Molecular Formula:C₃₂H₃₇NO₄
Molecular Weight:499.65
Hs Code.:

Synonyms:Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Suppliers and Price of Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

There total 8 articles about Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77-78-1
dimethyl sulfate

: 146903-02-8
(S)-2,2-Dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoic acid

: 155099-10-8
Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Guidance literature:: With potassium carbonate; In acetone; Ambient temperature;
DOI:10.1021/jo00084a037

Reference yield:

: 31952-16-6
2,2-dibenzyl-1,3-propanediol

: 155099-10-8
Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / CH₂Cl₂ / Ambient temperature

2: DMSO, oxalyl chloride, diisopropylethylamine / CH₂Cl₂ / -78 deg C, 30 min then warm to room temp.

4: 73 percent / Jones' reagent / acetone / 0.5 h / 0 °C

5: 92 percent / K₂CO₃ / acetone / Ambient temperature

With jones' reagent; oxalyl dichloride; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetone;
DOI:10.1021/jo00084a037

Reference yield:

: 108385-55-3
2(S)-<(tert-butoxycarbonyl)amino>-3-phenyl-1-(phenylsulphonyl)propane

: 155099-10-8
Methyl (S)-2,2-dibenzyl-5-<(tert-butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoate

Guidance literature:: Multi-step reaction with 3 steps

2: 73 percent / Jones' reagent / acetone / 0.5 h / 0 °C

3: 92 percent / K₂CO₃ / acetone / Ambient temperature

With jones' reagent; potassium carbonate; In acetone;
DOI:10.1021/jo00084a037