Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane

Base Information

• Chemical Name: Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane
• CAS No.: 196510-44-8
• Molecular Formula: C₂₆H₃₃BrO₂SSi
• Molecular Weight: 517.602

Synonyms:Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane

Chemical Property of Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane

Chemical Property:

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Technology Process of Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane

There total 1 articles about Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

bromomethyldimethylsilyl chloride (16532-02-8) + C23H26O2S → Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane (196510-44-8)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; 1.) -78 deg C, 2.5 h, 2.) 25 deg C, 12 h;

DOI:10.1021/jo970445e

Reference yield: 63.0%

Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane (196510-44-8) → (5-Cyclohex-1-enyl-pent-1-ynyl)-benzene

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Heating;

DOI:10.1021/jo970445e

Reference yield:

Bromomethyl-dimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane (196510-44-8) → Trimethyl-{2-[1-(5-phenyl-pent-4-ynyl)-cyclohexanesulfonyl]-phenyl}-silane

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 6h; Heating;

DOI:10.1021/jo970445e

upstream raw materials:

bromomethyldimethylsilyl chloride

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