4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate

Base Information

• Chemical Name: 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate
• CAS No.: 1057314-07-4
• Molecular Formula: C₂₁H₁₇Cl₂F₃N₂O₄S
• Molecular Weight: 521.344

Synonyms:4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate

Chemical Property of 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate

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Technology Process of 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate

There total 1 articles about 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-chloro-2-methylphenyl)-4-methyl-5-(4-{[(3,3,3-trifluoropropyl)sulfonyl]oxy}phenyl)-1H-pyrazole-3-carboxylic acid (921591-21-1) → 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate (1057314-07-4)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.833333h;

Reference yield:

4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate (1057314-07-4) + N-aminopiperidine hydrochloride (63234-70-8) → 4-{1-(4-chloro-2-methylphenyl)-4-methyl-3-[(piperidin-1-ylamino)carbonyl]-1H-pyrazol-5-yl}phenyl 3,3,3-trifluoropropane-1-sulfonate

Guidance literature:

With potassium carbonate; In dichloromethane; water; at 20 ℃; for 1.5h;

Reference yield:

cis-2-aminocyclohexanol hydrochloride + 4-[3-(chlorocarbonyl)-1-(4-chloro-2-methylphenyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate (1057314-07-4) → 4-[1-(4-chloro-2-methylphenyl)-3-({[(1R,2S)-2-hydroxycyclohexyl]amino}carbonyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate + 4-[1-(4-chloro-2-methylphenyl)-3-({[(1S,2R)-2-hydroxycyclohexyl]amino}carbonyl)-4-methyl-1H-pyrazol-5-yl]phenyl 3,3,3-trifluoropropane-1-sulfonate

Guidance literature:

With potassium carbonate; In dichloromethane; water;

upstream raw materials:

1-(4-chloro-2-methylphenyl)-4-methyl-5-(4-{[(3,3,3-trifluoropropyl)sulfonyl]oxy}phenyl)-1H-pyrazole-3-carboxylic acid

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