C₁₇H₂₆O₃Si

Base Information

• Chemical Name: C₁₇H₂₆O₃Si
• CAS No.: 1383440-57-0
• Molecular Formula: C₁₇H₂₆O₃Si
• Molecular Weight: 306.477
• Mol file: 1383440-57-0.mol

Synonyms:C₁₇H₂₆O₃Si

Chemical Property of C₁₇H₂₆O₃Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₇H₂₆O₃Si

There total 2 articles about C₁₇H₂₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl(2-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)silane (853955-58-5) + methyl 2-heptynoate (18937-78-5) → C17H26O3Si (1383440-57-0)

Guidance literature:

dimethyl(2-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)silane; methyl 2-heptynoate; With platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane; In dichloromethane; at 23 ℃; for 24h;

With toluene-4-sulfonic acid; In methanol; at 23 ℃; for 1h; regioselective reaction;

DOI:10.1021/ol301300r

Reference yield:

dimethyl(2-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)silane (853955-58-5) + methyl 2-heptynoate (18937-78-5) → C17H26O3Si + C17H26O3Si (1383440-57-0)

Guidance literature:

dimethyl(2-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)silane; methyl 2-heptynoate; With platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane; In dichloromethane; at 23 ℃;

With toluene-4-sulfonic acid; In methanol; at 23 ℃; for 2h; regioselective reaction;

DOI:10.1021/ol301300r

Reference yield: 96.0%

4-iodobenzonitrile (3058-39-7) + C17H26O3Si (1383440-57-0) → C15H17NO2 (1383440-64-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver(l) oxide; In 1,4-dioxane; at 50 ℃; for 8h; Inert atmosphere;

DOI:10.1021/ol301300r

upstream raw materials:

dimethyl(2-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)silane

methyl 2-heptynoate

Downstream raw materials:

C₁₄H₁₇NO₄

C₁₄H₁₈O₂

C₁₅H₂₀O₃

C₁₅H₁₇NO₂

Refernces