O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate
• CAS No.: 1070883-64-5
• Molecular Formula: C₁₆H₂₄N₄O₆
• Molecular Weight: 368.39

Synonyms:O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate

Chemical Property of O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate

Chemical Property:

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Technology Process of O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate

There total 1 articles about O⁽²⁾-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-(2-bromomethyl-4-nitrophenoxy)tetrahydropyran (141456-02-2) + sodium N,N-(diethylamino)diazen-1-ium-1,2-diolate (138475-09-9) → O(2)-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate (1070883-64-5)

Guidance literature:

With 15-crown-5; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1021/ol801883f

Reference yield: 90.0%

O(2)-((5-nitro-2-(tetrahydropyran-2-yloxy)phenyl)methyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate (1070883-64-5) → O(2)-(2-hydroxy-5-nitrobenzyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate (1070883-62-3)

Guidance literature:

With hydrogenchloride; In diethyl ether;

DOI:10.1021/ol801883f

upstream raw materials:

2-(2-bromomethyl-4-nitrophenoxy)tetrahydropyran

sodium N,N-(diethylamino)diazen-1-ium-1,2-diolate

Downstream raw materials:

O⁽²⁾-(2-hydroxy-5-nitrobenzyl)-1-( N,N-diethylamino)diazen-1-ium-1,2-diolate

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