(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

Base Information

Chemical Name:(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester
CAS No.:180468-21-7
Molecular Formula:C₁₈H₂₂N₂O₈S
Molecular Weight:426.447
Hs Code.:

Synonyms:(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

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Chemical Property of (2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

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Technology Process of (2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

There total 3 articles about (2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[(2R,3S)-2-Methoxysulfinyl-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-2-enoic acid methyl ester

: 180468-21-7
(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

Guidance literature:: With formic acid; dihydrogen peroxide; In dichloromethane; at 20 ℃; for 10h; Yield given;

Reference yield:

: 81651-28-7
(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphinic acid

: 180468-21-7
(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 2 h / 25 °C

2: 1 h / 25 °C

3: 30percent aq. H₂O₂, formic acid / CH₂Cl₂ / 10 h / 20 °C

With formic acid; thionyl chloride; dihydrogen peroxide; In dichloromethane;

Reference yield:

: 2-[(2R,3S)-2-Chlorosulfinyl-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-2-enoic acid methyl ester

: 180468-21-7
(2R,3S)-3-phenoxyacetamido-1-(1'-methyloxycarbonyl-2'-methyl-prop-1'-enyl)-4-oxoazetidine-2-sulphonic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / 25 °C

2: 30percent aq. H₂O₂, formic acid / CH₂Cl₂ / 10 h / 20 °C

With formic acid; dihydrogen peroxide; In dichloromethane;