C₂₂H₂₂ClNO₄

Base Information

Chemical Name:C₂₂H₂₂ClNO₄
CAS No.:1311388-39-2
Molecular Formula:C₂₂H₂₂ClNO₄
Molecular Weight:399.874
Hs Code.:

C<sub>22</sub>H<sub>22</sub>ClNO<sub>4</sub>

Synonyms:C₂₂H₂₂ClNO₄

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Chemical Property of C₂₂H₂₂ClNO₄

Chemical Property:

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Technology Process of C₂₂H₂₂ClNO₄

There total 6 articles about C₂₂H₂₂ClNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1311388-61-0
C₂₂H₂₀ClNO₄

: 1311388-39-2
C₂₂H₂₂ClNO₄

Guidance literature:: With sodium tetrahydroborate; nickel dichloride; In methanol; 1,2-dimethoxyethane; at 20 ℃; for 0.5h;
DOI:10.1002/adsc.201100034

Reference yield:

: 1333247-76-9
5-((4-chlorophenyl)(hydroxy)methyl)-N-(3,5-dimethoxyphenyl)-N-ethylfuran-2-carboxamide

: 1311388-39-2
C₂₂H₂₂ClNO₄

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; acetic acid / toluene / 1 h / 100 °C

2: sodium tetrahydroborate; nickel dichloride / methanol; 1,2-dimethoxyethane / 0.5 h / 20 °C

With sodium tetrahydroborate; copper(ll) sulfate pentahydrate; acetic acid; nickel dichloride; In methanol; 1,2-dimethoxyethane; toluene; 1: Friedel Crafts alkylation;
DOI:10.1002/adsc.201100034

Reference yield:

: 65650-09-1
5-(4-chloro-benzoyl)-furan-2-carboxylic acid

: 1311388-39-2
C₂₂H₂₂ClNO₄

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 3 h / Reflux

2: triethylamine / tetrahydrofuran

3: sodium tetrahydroborate / methanol / 20 °C

4: copper(ll) sulfate pentahydrate; acetic acid / toluene / 1 h / 100 °C

5: sodium tetrahydroborate; nickel dichloride / methanol; 1,2-dimethoxyethane / 0.5 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; copper(ll) sulfate pentahydrate; acetic acid; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; toluene; 4: Friedel Crafts alkylation;
DOI:10.1002/adsc.201100034