phenylsulfurimidoyl difluoride

Base Information

• Chemical Name: phenylsulfurimidoyl difluoride
• CAS No.: 658-33-3
• Molecular Formula: C₆H₅F₂NOS
• Molecular Weight: 177.175
• Mol file: 658-33-3.mol

Synonyms:phenylsulfurimidoyl difluoride

Chemical Property of phenylsulfurimidoyl difluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of phenylsulfurimidoyl difluoride

There total 2 articles about phenylsulfurimidoyl difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

aniline (62-53-3) → phenylsulfurimidoyl difluoride (658-33-3)

Guidance literature:

With thionyl tetrafluoride; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Sealed tube;

DOI:10.1002/anie.201712145

Reference yield:

→ phenylsulfurimidoyl difluoride (658-33-3)

Guidance literature:

entspr.Amin, SOF4;

Reference yield: 81.0%

phenylsulfurimidoyl difluoride (658-33-3) + phenyllithium (591-51-5) → N-(phenyl)benzenesulfonimidoyl fluoride (83706-31-4)

Guidance literature:

In dibutyl ether; at -78 ℃; for 0.0833333h; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.201712145

upstream raw materials:

aniline

Downstream raw materials:

ethyl phenylamidosulfate

4-Chlor-phenyliminoschwefeloxydifluorid

N-(phenyl)benzenesulfonimidoyl fluoride

(±)-methyl(phenyl)(phenylimino)-λ⁶-sulfanone