5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

Base Information

Chemical Name:5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone
CAS No.:64065-70-9
Molecular Formula:C₄₆H₄₈O₂₄
Molecular Weight:984.873
Hs Code.:

Synonyms:5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

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Chemical Property of 5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

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Technology Process of 5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

There total 2 articles about 5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₅₄O₁₄

: 108-24-7
acetic anhydride

: 64065-70-9
5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

: 5,7,4'-triacetoxy-6-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-8-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)flavone

Guidance literature:: C₅₄H₅₄O₁₄; In methanol; Reflux;

With palladium 10% on activated carbon; hydrogen;

acetic anhydride; Further stages;
DOI:10.1016/j.carres.2010.04.001

Reference yield:

: C₄₂H₄₄O₂₂

: 108-24-7
acetic anhydride

: 64065-70-9
5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

Guidance literature:: With pyridine;
DOI:10.1039/c0ob00011f

Reference yield: 85.0%

: 64065-70-9
5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone

: 35927-38-9
6-(C-β-D-xylopyranosyl)-8-(C-β-D-glucopyranosyl)-4',5,7-trihydroxyflavone

Guidance literature:: 5,7,4'-triacetoxy-6-C-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-8-C-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)flavone; With sodium methylate; In methanol; at 25 ℃;

In methanol;
DOI:10.1039/c0ob00011f