C₁₉H₃₀O₇

Base Information

• Chemical Name: C₁₉H₃₀O₇
• CAS No.: 1393086-97-9
• Molecular Formula: C₁₉H₃₀O₇
• Molecular Weight: 370.443
• Mol file: 1393086-97-9.mol

Synonyms:C₁₉H₃₀O₇

Chemical Property of C₁₉H₃₀O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₃₀O₇

There total 3 articles about C₁₉H₃₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

C15H24O6 (1393086-96-8) + Triethyl orthoacetate (78-39-7) → C19H30O7 (1393086-97-9)

Guidance literature:

With propionic acid; at 190 - 200 ℃; for 40h;

DOI:10.1016/j.tetlet.2012.06.001

Reference yield:

C20H32O2Si → C19H30O7 (1393086-97-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 10 h / 25 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 25 °C

3: diphenylether / 0.25 h / 210 °C

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 - 25 °C

5: propionic acid / 40 h / 190 - 200 °C

With tetrabutyl ammonium fluoride; acetic acid; propionic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diphenylether; dichloromethane; 3: retro-Diels-Alder reaction;

DOI:10.1016/j.tetlet.2012.06.001

Reference yield:

C21H38O6Si (1393086-95-7) → C19H30O7 (1393086-97-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 - 25 °C

2: propionic acid / 40 h / 190 - 200 °C

With tetrabutyl ammonium fluoride; acetic acid; propionic acid; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2012.06.001

upstream raw materials:

C₂₁H₃₈O₆Si

C₁₅H₂₄O₆

Triethyl orthoacetate

Downstream raw materials:

C₂₀H₃₃O₉P