(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

Base Information

Chemical Name:(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide
CAS No.:412306-77-5
Molecular Formula:C₁₈H₂₀N₂O₅
Molecular Weight:344.367
Hs Code.:

Synonyms:(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

Chemical Property:

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Technology Process of (3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

There total 6 articles about (3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55149-84-3
2-nitroveratraldehyde

: 412306-77-5
(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

Guidance literature:: Multi-step reaction with 5 steps

1: alcoholic KOH-solution

2: benzene; PCl₅ / 0 °C

3: alcohol

4: methanol; hydrogen chloride; diethyl ether / 0 °C / Erwaermen des entstandenen Iminomethylaetherhydrochlorids erst mit Wasser, dann mit Salzsaeure

5: phosphorus pentachloride / durch Schuetteln des entstandenen Chlorids mit β-Phenaethylamin und verd. Natronlauge

With hydrogenchloride; methanol; potassium hydroxide; diethyl ether; ethanol; phosphorus pentachloride; benzene;

Reference yield:

: 70400-74-7
(3,4-dimethoxy-2-nitro-phenyl)-acetic acid

: 412306-77-5
(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

Guidance literature:: With phosphorus pentachloride; durch Schuetteln des entstandenen Chlorids mit β-Phenaethylamin und verd. Natronlauge;

Reference yield:

: 43027-36-7
3,4-dimethoxy-2-nitrobenzylchloride

: 412306-77-5
(3,4-dimethoxy-2-nitro-phenyl)-acetic acid phenethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: alcohol

2: methanol; hydrogen chloride; diethyl ether / 0 °C / Erwaermen des entstandenen Iminomethylaetherhydrochlorids erst mit Wasser, dann mit Salzsaeure

3: phosphorus pentachloride / durch Schuetteln des entstandenen Chlorids mit β-Phenaethylamin und verd. Natronlauge

With hydrogenchloride; methanol; diethyl ether; ethanol; phosphorus pentachloride;