1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

Base Information

Chemical Name:1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)
CAS No.:255851-93-5
Molecular Formula:C₅₈H₆₂O₁₅P₂
Molecular Weight:1061.07
Hs Code.:

Synonyms:1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

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Technology Process of 1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

There total 6 articles about 1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: Phosphoric acid dibenzyl ester (1R,2S,3S,4R,5S,6R)-2,3,5-tris-benzyloxymethoxy-6-(bis-benzyloxy-phosphoryloxy)-4-(4-methoxy-benzyloxy)-cyclohexyl ester

: 255851-93-5
1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 23 ℃; for 4h;
DOI:10.1016/S0040-4039(99)01877-8

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 255851-93-5
1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / CH₂Cl₂ / 2 h / 23 °C

2: m-CPBA / 1 h / -40 °C

3: 80 percent / DDQ; H₂O / CH₂Cl₂ / 4 h / 23 °C

With 1H-tetrazole; water; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; 1: phosphorylation / 2: Oxidation / 3: ether cleavage;
DOI:10.1016/S0040-4039(99)01877-8

Reference yield:

: (1S,2S,3R,4S,5S,6R)-3,4,6-Tris-benzyloxymethoxy-5-(4-methoxy-benzyloxy)-cyclohexane-1,2-diol

: 255851-93-5
1D-2,3,6-tris-O-(benzyloxymethyl)-myo-inositol 4,5-bis(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / CH₂Cl₂ / 2 h / 23 °C

2: m-CPBA / 1 h / -40 °C

3: 80 percent / DDQ; H₂O / CH₂Cl₂ / 4 h / 23 °C

With 1H-tetrazole; water; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; 1: phosphorylation / 2: Oxidation / 3: ether cleavage;
DOI:10.1016/S0040-4039(99)01877-8