9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

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Chemical Name:9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride
CAS No.:1266100-38-2
Molecular Formula:C₃₀H₃₀N₂O₅*ClH
Molecular Weight:535.04
Hs Code.:

Synonyms:9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

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Chemical Property of 9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

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Technology Process of 9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

There total 6 articles about 9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1266100-37-1
C₃₅H₃₈N₂O₇

: 1266100-38-2
9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield:

: 1264243-44-8,1865786-36-2
tert-butyl (3R,5S)-5-(hydroxymethyl)pyrrolidin-3-ylcarbamate hydrochloride

: 1266100-38-2
9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / 1,4-dioxane; water

2: triphenylphosphine; diethylazodicarboxylate / toluene; benzene / 16 h / 0 - 20 °C

3: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

With hydrogenchloride; sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; water; toluene; benzene; 2: Mitsunobu reaction;

Reference yield:

: 16446-73-4
3-(chlorocarbonyl)phenyl acetate

: 1266100-38-2
9H-fluoren-9-ylmethyl (2S,4R)-2-(3-[(allyloxy)-carbonyl]phenoxymethyl)-4-aminotetrahydro-1H-pyrrole-1-carboxylate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

2: 1-amino-3-(dimethylamino)propane / tetrahydrofuran / 3 h / 0 - 20 °C

3: triphenylphosphine; diethylazodicarboxylate / toluene; benzene / 16 h / 0 - 20 °C

4: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

With hydrogenchloride; triethylamine; 1-amino-3-(dimethylamino)propane; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene; benzene; 3: Mitsunobu reaction;