tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

Base Information

Chemical Name:tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate
CAS No.:1345673-34-8
Molecular Formula:C₃₃H₄₆BNO₄
Molecular Weight:531.544
Hs Code.:

Synonyms:tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

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Chemical Property of tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

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Technology Process of tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

There total 4 articles about tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 936116-57-3
N-(diphenylmethylene)-DL-homoallylglycine tert-butyl ester

: 1236275-93-6
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-iodobutane

: 1345673-34-8
tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

Guidance literature:: N-(diphenylmethylene)-DL-homoallylglycine tert-butyl ester; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-iodobutane; In tetrahydrofuran; at -78 - 20 ℃; for 16h;

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1345673-34-8
tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 16 h / Inert atmosphere

2.1: sodium iodide / acetone / 4 h / 50 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

3.2: 16 h / -78 - 20 °C

With sodium hexamethyldisilazane; sodium iodide; In tetrahydrofuran; acetone;

Reference yield:

: 124215-50-5
2-(4-bromobutyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1345673-34-8
tert-butyl 2-(diphenylmethyleneamino)-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butyl)hex-5-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide / acetone / 4 h / 50 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: 16 h / -78 - 20 °C

With sodium hexamethyldisilazane; sodium iodide; In tetrahydrofuran; acetone;