5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

Base Information

Chemical Name:5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole
CAS No.:1613810-50-6
Molecular Formula:C₄₄H₄₈N₂O₂
Molecular Weight:636.877
Hs Code.:

Synonyms:5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

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Chemical Property of 5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

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Technology Process of 5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

There total 4 articles about 5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

: 111-25-1
1-bromo-hexane

: 1613810-50-6
5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: 6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

1-bromo-hexane; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.24820/ark.5550190.p010.557

Reference yield:

: 1613810-44-8
5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

: 1613810-50-6
5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 10 - 20 ℃; for 2h; Reagent/catalyst; Solvent; Temperature;
DOI:10.1016/j.tet.2014.04.093

Reference yield:

: 120-72-9
indole

: 1613810-50-6
5,11-dihexyl-6,12-bis(4-methoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; tetrafluoroboric acid / water; acetonitrile / 3 h / 15 - 20 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 15 h / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 2 h / 10 - 20 °C

With tetrafluoroboric acid; tetra-(n-butyl)ammonium iodide; pyridinium chlorochromate; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2014.04.093