L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Base Information

Chemical Name:L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride
CAS No.:127132-41-6
Molecular Formula:C₂₃H₃₅N₃O₅*ClH
Molecular Weight:470.009
Hs Code.:

Synonyms:L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Suppliers and Price of L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

There total 10 articles about L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127132-40-5
N-(tert-butoxycarbonyl)-L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester

: 127132-41-6
L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 2h; Ambient temperature;
DOI:10.1021/jm00168a015

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 127132-41-6
L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / methanol; tetrahydrofuran / 20 h / Ambient temperature

2: 72 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, 1-hydroxybenzotriazole, Et₃N / dimethylformamide / 24 h / Ambient temperature

3: 96 percent / HCl / dioxane / 2 h / Ambient temperature

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00168a015

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 127132-41-6
L-valyl-O'-(prop-2-enyl)-L-tyrosyl-L-valine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, 1-hydroxybenzotriazole, Et₃N / dimethylformamide / 24 h / Ambient temperature

2: 96 percent / HCl / dioxane / 2 h / Ambient temperature

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00168a015