(Rs)-2,4,6-trimethylbenzenesulfinamide

Base Information

• Chemical Name: (Rs)-2,4,6-trimethylbenzenesulfinamide
• CAS No.: 446021-73-4
• Molecular Formula: C₉H₁₃NOS
• Molecular Weight: 183.274
• Hs Code.: 2930909899

Synonyms:(Rs)-2,4,6-trimethylbenzenesulfinamide

Chemical Property of (Rs)-2,4,6-trimethylbenzenesulfinamide

Chemical Property:

• Melting Point: 116-118 °C
• Boiling Point: 350.1±52.0 °C(Predicted)
• Density: 1.20±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

(R)-2,4,6-Trimethylbenzenesulfinamide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (Rs)-2,4,6-trimethylbenzenesulfinamide

There total 12 articles about (Rs)-2,4,6-trimethylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

quinine (Rs)-2,4,6-trimethylbenzenesulfinate (1351958-44-5) → (Rs)-2,4,6-trimethylbenzenesulfinamide (446021-73-4)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 0.5h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/jo201825b

Reference yield: 80.0%

2,4,6-Trimethyl-benzenesulfinic acid (1R,2S)-1-(2,4,6-trimethyl-benzenesulfonylamino)-indan-2-yl ester → (Rs)-2,4,6-trimethylbenzenesulfinamide (446021-73-4)

Guidance literature:

With sodium hexamethyldisilazane; lithium; ferric nitrate; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1021/ja0200692

Reference yield: 72.0%

C25H29NO4S2 (1011794-50-5) → (Rs)-2,4,6-trimethylbenzenesulfinamide (446021-73-4)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

DOI:10.1016/j.tetlet.2007.12.067

upstream raw materials:

N-chloroacetyl-2,4,6-trimethylbenzenesulfinamide

2,4,6-trimethylbenzenesulphinamide

C₂₅H₂₉NO₄S₂

(2S,4R)-5,5-dimethyl-4-phenyl-N-tosyl-1,2,3-oxathiazolidine 2-oxide

Downstream raw materials:

(R_S,E)-N-benzylidene-2,4,6-trimethylbenzenesulfinamide

N-(3-phenyl-allylidene)-2,4,6-trimethylphenylsulfinamide

(R)-1-((R_S)-mesitylsulfinyl)-4-methylene-2-phenylpyrrolidine

(S)-1-((R_S)-mesitylsulfinyl)-4-methylene-2-phenylpyrrolidine

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