(-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

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Chemical Name:(-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol
CAS No.:146205-34-7
Molecular Formula:C₃₂H₃₃NO₅
Molecular Weight:511.618
Hs Code.:

Synonyms:(-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

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Chemical Property of (-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

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Technology Process of (-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

There total 2 articles about (-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 146205-33-6
(1R,2S)-1-(3,4-Bis-benzyloxy-phenyl)-2-methylamino-propan-1-ol

: 146205-34-7
(-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

Guidance literature:: With sodium hydrogencarbonate; sodium chloride; In water; ethyl acetate; for 6h; Ambient temperature;
DOI:10.1021/jo00057a050

Reference yield:

: 146205-32-5
(-)-(4S,5R)-4-methyl-5-<3',4'-bis(phenylmethoxy)phenyl>-2-oxazolidinone

: 146205-34-7
(-)-(αR,βS)-N-(benzyloxycarbonyl)-3,4-bis(phenylmethoxy)-α-<1-(methylamino)ethyl>benzenemethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / LiAlH₄ / tetrahydrofuran / Heating

2: 80 percent / NaHCO₃, NaCl / ethyl acetate; H₂O / 6 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydrogencarbonate; sodium chloride; In tetrahydrofuran; water; ethyl acetate;
DOI:10.1021/jo00057a050