phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Base Information

Chemical Name:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside
CAS No.:1030632-52-0
Molecular Formula:C₃₇H₆₄O₉Si₂
Molecular Weight:709.081
Hs Code.:

phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Synonyms:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

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Chemical Property of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

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Technology Process of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

There total 1 articles about phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1030632-48-4
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2R,6S)-5,6-dihydro-6-methyl-5-oxo-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: 1030632-52-0
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Guidance literature:: With sodium tetrahydroborate; cerium(III) chloride; In methanol; dichloromethane; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol800697k

Reference yield: 97.0%

: 1030632-52-0
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5R,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: 62-23-7
4-nitro-benzoic acid

: 1030632-56-4
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5S,6S)-5,6-dihydro-5-(p-nitrobenzoyloxy)-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol800697k