[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Base Information

Chemical Name:[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester
CAS No.:209412-73-7
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Suppliers and Price of [1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

There total 8 articles about [1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73323-82-7
2-(N-Methyl-N-phenylamino)-benzoic acid

: 209412-73-7
[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / K₂CO₃ / dimethylformamide / 12 h / Ambient temperature

2: 83 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

3: 50 percent / CrO₃, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

4: 86 percent / NH₂OH*HCl, pyridine / ethanol / 0.5 h / Heating

5: 91 percent / NaOH / H₂O / 16 h / Heating

6: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With pyridine; chromium(VI) oxide; sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; potassium carbonate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/a800868j

Reference yield:

: 117296-15-8
(2-(methyl(phenyl)amino)phenyl)methanol

: 209412-73-7
[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / CrO₃, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: 86 percent / NH₂OH*HCl, pyridine / ethanol / 0.5 h / Heating

3: 91 percent / NaOH / H₂O / 16 h / Heating

4: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With pyridine; chromium(VI) oxide; sodium hydroxide; hydroxylamine hydrochloride; 1,1'-carbonyldiimidazole; In ethanol; dichloromethane; water;
DOI:10.1039/a800868j

Reference yield:

: 100-61-8
N-methylaniline

: 209412-73-7
[1-[2-(Methyl-phenyl-amino)-phenyl]-meth-(E)-ylideneaminooxy]-ethaneperoxoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / K₂CO₃, Cu / 3 h / 200 °C

2: 94 percent / K₂CO₃ / dimethylformamide / 12 h / Ambient temperature

3: 83 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

4: 50 percent / CrO₃, pyridine / CH₂Cl₂ / 1 h / Ambient temperature

5: 86 percent / NH₂OH*HCl, pyridine / ethanol / 0.5 h / Heating

6: 91 percent / NaOH / H₂O / 16 h / Heating

7: 1.) CDI / 1.) THF, r.t., 1 h, 2.) THF, light petroleum, 0-5 deg C, 4 h

With pyridine; chromium(VI) oxide; sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; copper; potassium carbonate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/a800868j