Technology Process of C30H29N3
There total 4 articles about C30H29N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / 3 h / Molecular sieve; Reflux
2: palladium diacetate; potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / butan-1-ol / 2 h / 80 °C / Inert atmosphere; Schlenk technique
3: sodium cyanoborohydride; formic acid / methanol; water / 1 h / Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; formic acid; palladium diacetate; sodium cyanoborohydride; toluene-4-sulfonic acid;
In
methanol; water; butan-1-ol;
2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.molcata.2012.12.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / butan-1-ol / 2 h / 80 °C / Inert atmosphere; Schlenk technique
2: sodium cyanoborohydride; formic acid / methanol; water / 1 h / Reflux
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; formic acid; palladium diacetate; sodium cyanoborohydride;
In
methanol; water; butan-1-ol;
1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.molcata.2012.12.008