1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane

Base Information

• Chemical Name: 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane
• CAS No.: 300854-48-2
• Molecular Formula: C₁₈H₂₂N₃OP
• Molecular Weight: 327.366

Synonyms:1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane

Chemical Property of 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane

Chemical Property:

Purity/Quality:

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Technology Process of 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane

There total 2 articles about 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N-Bis(2-chloroethyl)-N',N''-di(4-methylphenyl)phosphotriamidate (300854-51-7) → 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ5-phosphabicyclo[3.3.0]octane (300854-48-2)

Guidance literature:

With tetrabutylammomium bromide; sodium hydride; In tetrahydrofuran;

DOI:10.1055/s-2000-6421

Reference yield:

p-toluidine (106-49-0,12221-03-3) → 1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ5-phosphabicyclo[3.3.0]octane (300854-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / Et₃N

2: 90 percent / NaH; tetrabutylammonium bromide / tetrahydrofuran

With tetrabutylammomium bromide; sodium hydride; triethylamine; In tetrahydrofuran; 1: Substitution / 2: Cyclization;

DOI:10.1055/s-2000-6421

Reference yield:

1-Oxo-2,8-di(4-methylphenyl)-2,5,8-triaza-1λ5-phosphabicyclo[3.3.0]octane (300854-48-2) → N-p-tolyl-N'-(2-p-tolylamino-ethyl)-ethane-1,2-diamine; compound with GENERIC INORGANIC NEUTRAL COMPONENT

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 24h;

DOI:10.1055/s-2000-6421

upstream raw materials:

N-Bis(2-chloroethyl)-N',N''-di(4-methylphenyl)phosphotriamidate

p-toluidine

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