4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

Base Information

Chemical Name:4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one
CAS No.:1269632-20-3
Molecular Formula:C₂₆H₁₇N₃O₅S
Molecular Weight:483.504
Hs Code.:

Synonyms:4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

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Chemical Property of 4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

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Technology Process of 4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

There total 5 articles about 4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: ethyl 4-(bromomethyl)-2-(2-nitrophenyl)-9-(phenylsulfonyl)-9H-carbazole-3-carboxylate

: 1269632-20-3
4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; for 1h; Reflux;
DOI:10.1021/acs.orglett.8b03063

Reference yield: 92.0%

: 1269632-19-0
methyl 4-(bromomethyl)-2-(2'-nitrophenyl)-9-(phenylsulfonyl)carbazole-3-carboxylate

: 1269632-20-3
4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

Guidance literature:: With ammonia; In tetrahydrofuran; water; for 2h; Reflux; Inert atmosphere;
DOI:10.1021/ol200094b

Reference yield:

: (E)-2-(2-nitrostyryl)-1H-indole

: 1269632-20-3
4-(2-nitrophenyl)-6-(phenylsulfonyl)-1,2-dihydropyrrolo[3,4-c]carbazol-3(6H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl hydrogen phosphate / ethyl acetate / 54 h / 110 °C / Sealed tube

1.2: air / 28 h / 130 °C / Sealed tube

2.1: sodium hydride / mineral oil; tetrahydrofuran / 4 h / 20 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1.5 h / 20 °C

4.1: ammonium hydroxide / tetrahydrofuran / 1 h / Reflux

With ammonium hydroxide; N-Bromosuccinimide; diphenyl hydrogen phosphate; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; tetrachloromethane; ethyl acetate; mineral oil;
DOI:10.1021/acs.orglett.8b03063