benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside
CAS No.:102794-19-4
Molecular Formula:C₂₇H₂₉Cl₆NO₁₀
Molecular Weight:740.246
Hs Code.:

Synonyms:benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Chemical Property of benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Technology Process of benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

There total 3 articles about benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3587-60-8
Benzyloxymethyl chloride

: 114827-03-1,102794-18-3
benzyl 2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

: 102794-19-4
benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: With tetramethylurea; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1248/cpb.33.4098

Reference yield:

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 102794-19-4
benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 4-dimethylaminopyridine / 2 h / Ambient temperature

2: 98 percent / 90percent acetic acid / H₂O / 0.25 h / 90 °C

3: 85 percent / tetramethylurea / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; acetic acid; tetramethylurea; In dichloromethane; water;
DOI:10.1248/cpb.33.4098

Reference yield:

: 102794-16-1
benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

: 102794-19-4
benzyl 6-O-benzyloxymethyl-2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 90percent acetic acid / H₂O / 0.25 h / 90 °C

2: 85 percent / tetramethylurea / CH₂Cl₂ / 16 h / Ambient temperature

With acetic acid; tetramethylurea; In dichloromethane; water;
DOI:10.1248/cpb.33.4098