C₃₆H₅₂BrNO₂Si

Base Information

Chemical Name:C₃₆H₅₂BrNO₂Si
CAS No.:1565829-58-4
Molecular Formula:C₃₆H₅₂BrNO₂Si
Molecular Weight:638.804
Hs Code.:

C<sub>36</sub>H<sub>52</sub>BrNO<sub>2</sub>Si

Synonyms:C₃₆H₅₂BrNO₂Si

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Chemical Property of C₃₆H₅₂BrNO₂Si

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Technology Process of C₃₆H₅₂BrNO₂Si

There total 1 articles about C₃₆H₅₂BrNO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 617-86-7
triethylsilane

: C₃₀H₃₆BrNO₂

: 1565829-58-4
C₃₆H₅₂BrNO₂Si

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In 5,5-dimethyl-1,3-cyclohexadiene; toluene; at 20 - 60 ℃; for 2.5h; enantiospecific reaction; Inert atmosphere;
DOI:10.1021/ja501142e

Reference yield: 96.0%

: 1565829-58-4
C₃₆H₅₂BrNO₂Si

: 1565829-42-6
C₃₆H₅₂BrNO₂Si

Guidance literature:: In para-xylene; at 175 ℃; for 23h; enantiospecific reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja501142e

Reference yield:

: 1565829-58-4
C₃₆H₅₂BrNO₂Si

: 1565829-50-6
C₂₈H₃₅NO

: (+)-tubingensin A

Guidance literature:: Multi-step reaction with 4 steps

1: para-xylene / 23 h / 175 °C / Schlenk technique; Inert atmosphere

2: sodium amide / tetrahydrofuran; tert-butyl alcohol / 3 h / 23 °C / Inert atmosphere

3: ethylene glycol; hydrogenchloride / tetrahydrofuran / 20.5 h / 55 °C / Inert atmosphere

4: sodium / toluene; isopropyl alcohol / 3 h / 0 - 23 °C / Inert atmosphere

With hydrogenchloride; sodium; sodium amide; ethylene glycol; In tetrahydrofuran; para-xylene; isopropyl alcohol; toluene; tert-butyl alcohol;
DOI:10.1021/ja501142e