(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

Base Information

Chemical Name:(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide
CAS No.:1297538-98-7
Molecular Formula:C₁₉H₁₂ClF₃N₂O₂
Molecular Weight:392.765
Hs Code.:

Synonyms:(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

Chemical Property:

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Technology Process of (E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

There total 3 articles about (E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1452-77-3
pyridine-2-carboxylic acid amide

: 1297538-97-6
(E)-2-(2-bromovinyl)-5-(4-chloro-3-(trifluoromethyl)phenyl)furan

: 1297538-98-7
(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

Guidance literature:: With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In toluene; for 7.5h; Inert atmosphere; Reflux;

Reference yield:

: 58110-58-0
5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-carbaldehyde

: 1297538-98-7
(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine; pyridine / 4 h / Reflux

2: Dess-Martin periodane; tetraethylammonium bromide / dichloromethane / 1.5 h / 20 °C

3: potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 7.5 h / Inert atmosphere; Reflux

With piperidine; pyridine; copper(l) iodide; tetraethylammonium bromide; potassium carbonate; Dess-Martin periodane; N,N`-dimethylethylenediamine; In dichloromethane; toluene;

Reference yield:

: 62806-38-6
(E)-3-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)acrylic acid

: 1297538-98-7
(E)-N-(2-(5-(4-chloro-3-(trifluoromethyl)phenyl)furan-2-yl)vinyl)picolinamide

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane; tetraethylammonium bromide / dichloromethane / 1.5 h / 20 °C

2: potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 7.5 h / Inert atmosphere; Reflux

With copper(l) iodide; tetraethylammonium bromide; potassium carbonate; Dess-Martin periodane; N,N`-dimethylethylenediamine; In dichloromethane; toluene;