Technology Process of C39H46N6O6
There total 8 articles about C39H46N6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C35H39N5O5;
With
hydrogenchloride;
In
1,4-dioxane; methanol;
N-(tert-butoxycarbonyl)-N-methyl-L-alanine;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: hydrogenchloride / 1,4-dioxane; methanol / 20 °C
1.2: 20 °C
2.1: triphenylphosphine; ozone / dichloromethane
3.1: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 20 °C
4.1: sodium hydrogencarbonate / 1,4-dioxane
5.1: lithium hydroxide / 1,4-dioxane
6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane
7.1: acetic acid / 10 h / 80 °C
8.1: hydrogenchloride / 1,4-dioxane; methanol
With
hydrogenchloride; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; ozone; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide;
palladium 10% on activated carbon;
In
1,4-dioxane; methanol; dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / isopropyl alcohol / 20 °C
2: sodium hydrogencarbonate / 1,4-dioxane
3: lithium hydroxide / 1,4-dioxane
4: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane
5: acetic acid / 10 h / 80 °C
6: hydrogenchloride / 1,4-dioxane; methanol
With
hydrogenchloride; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
palladium 10% on activated carbon;
In
1,4-dioxane; methanol; dichloromethane; isopropyl alcohol;