ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

Base Information

Chemical Name:ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate
CAS No.:1258209-20-9
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

Synonyms:ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

Suppliers and Price of ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

There total 1 articles about ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 61550-02-5
(furan-2-yloxy)-trimethylsilane

: 1258209-05-0
ethyl 3,3-dimethyl-6-oxocyclohex-1-enecarboxylate

: 1258209-20-9
ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

Guidance literature:: (furan-2-yloxy)-trimethylsilane; ethyl 3,3-dimethyl-6-oxocyclohex-1-enecarboxylate; With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at -78 ℃; Inert atmosphere;

With ammonium chloride; In dichloromethane; water; at -78 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201000504

Reference yield: 53.0%

: 1258209-20-9
ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate

: 814-49-3
diethyl chlorophosphate

: ethyl 2-(diethoxyphosphoryloxy)-5,5-dimethyl-6-(5-oxo-2,5-dihydrofuran-2-yl)cyclohex-1-enecarboxylate

Guidance literature:: ethyl 3,3-dimethyl-6-oxo-2-(5-oxo-2,5-dihydrofuran-2-yl)cyclohexanecarboxylate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

diethyl chlorophosphate; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201000504