N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline

Base Information

• Chemical Name: N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline
• CAS No.: 237058-17-2
• Molecular Formula: C₁₉H₃₁NO₂
• Molecular Weight: 305.461

Synonyms:N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline

Chemical Property of N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline

Chemical Property:

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Technology Process of N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline

There total 10 articles about N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C19H29NO2 (260996-00-7) → N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline (237058-17-2)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at -10 ℃;

DOI:10.1021/jo991544q

Reference yield: 80.0%

(3S,4aR,6aS,9R,10aR,11aS,11bS)-5-oxo-3,11b-epoxy-4a,6,6,9-tetramethyl-3,4,4a,11b-tetrahydroisoindolyl-<2,3-a>-perhydro-11,5a-benzoxazine (237058-08-1) → N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline (237058-17-2)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at -10 ℃; for 0.0833333h;

DOI:10.1021/jo9904462

Reference yield: 80.0%

C19H29NO2 → N-(8-mentholyl)-(3aS,6S,7aS)-3a,6-epoxy-7a-methyl-3a,6,7,7a-tetrahydroisoindoline (237058-17-2)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at -10 ℃;

DOI:10.1021/jo991544q

upstream raw materials:

(3S,4aR,6aS,9R,10aR,11aS,11bS)-5-oxo-3,11b-epoxy-4a,6,6,9-tetramethyl-3,4,4a,11b-tetrahydroisoindolyl-<2,3-a>-perhydro-11,5a-benzoxazine

C₁₉H₂₉NO₂

furfural

(-)-aminomenthol

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