1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

Base Information

Chemical Name:1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol
CAS No.:134159-85-6
Molecular Formula:C₁₃H₁₈N₆O₇
Molecular Weight:370.322
Hs Code.:

Synonyms:1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

Suppliers and Price of 1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

Chemical Property:

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Technology Process of 1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

There total 5 articles about 1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 134159-70-9
1L-1,3,4-tri-O-acetyl-5-O-benzoyl-6-O-methylsulfonyl-2-O-methyl-chiro-inositol

: 134159-85-6
1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

: 1D-1,3,5-tri-O-acetyl-2,4-diazido-2,4-dideoxy-6-O-methyl-chiro-inositol

: 134235-66-8
1D-1,2,3,5-tetra-O-acetyl-6-azido-6-deoxy-4-O-methyl-muco-inositol

Guidance literature:: With sodium azide; In ethanol; 2-methoxy-ethanol; for 6h; Heating;
DOI:10.1016/0008-6215(91)80116-5

Reference yield:

: 642-38-6
quebrachitol

: 134159-85-6
1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid monohydrate / dimethylformamide / 16 h / Ambient temperature

2: pyridine

3: 80percent aq. HOAc / 24 h / 55 °C

4: pyridine / 1.) RT, 2 h, 2.) RT, 15 h

5: 14 percent / NaN₃ / 2-methoxy-ethanol; ethanol / 6 h / Heating

With pyridine; sodium azide; toluene-4-sulfonic acid; acetic acid; In ethanol; 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80116-5

Reference yield:

: 17230-38-5,56193-51-2,96554-71-1
1L-1,3,4-tri-O-acetyl-2-O-methyl-chiro-inositol

: 134159-85-6
1D-1,2,3-tri-O-acetyl-5,6-diazido-5,6-dideoxy-4-O-methyl-chiro-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1.) RT, 2 h, 2.) RT, 15 h

2: 14 percent / NaN₃ / 2-methoxy-ethanol; ethanol / 6 h / Heating

With pyridine; sodium azide; In ethanol; 2-methoxy-ethanol;
DOI:10.1016/0008-6215(91)80116-5